Synthesis of 1,2,3,4‐Tetrahydrocarbazoles and Related Tricyclic Indoles.

Scott, Tricia L.; Burke, N. E.; Carrero‐Martinez, Grissell; Soederberg, Bjoern C. G.

doi:10.1002/chin.200720110

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“…Reaction of 2-methoxy-4-nitro-phenylhydrazine with cyclohexanone in the presence of acetic acid was MW irradiation at 100 W at the temperature 140 0 C give 6-nitro, 8-methoxy 1,2,3,4-tetrahydrocarbazole 35 (Scheme 11) [33]. The yield of the product (35) was found 80 %.…”

Section: Vera Barbieri and Maria Grazia Ferlin Reported Mw Assisted Synthesis Of Substituted 1234tetrahydrocarbazolesmentioning

confidence: 99%

“…Figure 13 Synthesis of substituted 1,2,3,4-tetrahydrocarbazole (38 a-i) 3.3. Synthesis of 1,2,3,4-tetrahydrocarbazoles from 2-(2-nitrophenyl)-2-cyclohexene-1-ones Tricia L. Scott et al and coworkers reported synthesis of 1,2,3,4-tetrahydrocarbazoles (1, 1a-1e) from reduction of 2-(2-nitrophenyl)-2-cyclohexene-1-ones (39 a-f) using palladium on carbon under 1 atm of hydrogen gas at ambient temperature[35] (Scheme 13). The yield of the reaction was found 62-94 %.…”

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confidence: 99%

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A review on synthesis methods of tricyclic 1,2,3,4-tetrahydrocarbazoles

Kumar¹,

Kumar²,

Chowdhary³

2022

World J. Adv. Res. Rev.

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In this review article, we discussed old to new synthetic methods used for the preparation of 1,2,3,4-Tetrahydrocarbazole (THCz) based on reported literature. Around the worldwide, various researchers energetically reported new synthetic methods for tetrahydrocarbazoles preparation using conventional method or microwave method or use of catalyst. This review will be helpful to synthetic and medicinal chemist to find selective method for the preparation of 1,2,3,4-Tetrahydrocarbazoles with good percentage yield and less time. This review will also useful to medicinal chemist to design new biologically active tetrahydrocarbazoles based on reported synthetic methods.

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Section: Vera Barbieri and Maria Grazia Ferlin Reported Mw Assisted Synthesis Of Substituted 1234tetrahydrocarbazolesmentioning

confidence: 99%

mentioning

confidence: 99%