2024
DOI: 10.1039/d4nj03285c
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Synthesis of 3′H-spiro[cyclohexane-1,1′-isobenzofuran]-2,5-dien-4-one and Skeleton construction of a type D spirobisnaphthalene structure via dearomatization by a high-valence iodine reagent and Diels–Alder reaction

Haoyun Ma,
Xinkun An,
Tingting Zhang
et al.

Abstract: The core skeleton syntheses 3’H-spiro[cyclohexane-1,1’-isobenzofuran]-2,5- dien-4-one and their derivatives (3a-3w) of spirobisnaphthalene urnucratins, plecmillins and lignan kadsulignan, were explored using the Suzuki–Miyaura coupling product biphenols as the precursors and the...

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