Org. Chem. Front.
 2024
DOI: 10.1039/d4qo01632g
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Synthesis of [4.6] spirocarbocycles: a base-promoted ring-expansion and subsequent I2-mediated regioselective spirocyclization protocol

Nana Fei,
Zongkang Wang,
Peng He
et al.

Abstract: An efficient protocol for the synthesis of [4.6] spirocarbocycles has been developed. This process is realized through the sequential K2CO3-promoted C−C σ-bond cleavage of cyclic ketoesters and an I2-mediated selective...

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