Synthesis of a Water‐Soluble Pd‐Based Catalyst with a Thymine‐Modified β‐Cyclodextrin Ligand for Suzuki Coupling Reactions
Rui Li,
Mengting Li,
Caihong Jiao
et al.
Abstract:Herein, the synthesis and crystal structure identification of thymine‐modified β‐cyclodextrin (mono‐(6‐Thymine‐6‐deoxy)‐β‐CD, Thy‐CD) are reported. The catalyst system (Pd@Thy‐CD) was prepared by using the thymine‐modified β‐cyclodextrin as ligand and palladium acetate (Pd(OAc)2) as palladium source. The as‐obtained Pd@Thy‐CD catalyst was characterized by NMR, IR, SEM, and XPS analysis. The catalyst can efficiently catalyze the aqueous phase Suzuki coupling reaction in situ. Under mild reaction conditions, the… Show more
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