Synthesis of Anthracene-9-C
            <sub>1</sub>
            <sup>14</sup>

Stevens, W. H.; Holland, D.

doi:10.1126/science.112.2920.718

Science

1950

DOI: 10.1126/science.112.2920.718

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Synthesis of Anthracene-9-C ₁ ¹⁴

W. H. Stevens

D. Holland

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1979

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Cited by 4 publications

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“…using thionyl chloride [14] and the resulting anhydride, 1, was converted to in 56% yield by bromination using bromine in chlorosulfonic acid [15].…”

mentioning

confidence: 99%

Synthesis of ¹⁴C‐labeled flame retardants. ¹⁴C‐labeled‐tetrabromophthalic anhydride and tetrabromobisphenol‐A

Susan¹,

Ebert²,

Duncan³

1979

Labelled Comp Radiopharmac

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“…using thionyl chloride [14] and the resulting anhydride, 1, was converted to in 56% yield by bromination using bromine in chlorosulfonic acid [15].…”

mentioning

confidence: 99%

Synthesis of ¹⁴C‐labeled flame retardants. ¹⁴C‐labeled‐tetrabromophthalic anhydride and tetrabromobisphenol‐A

Susan¹,

Ebert²,

Duncan³

1979

Labelled Comp Radiopharmac

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Synthesis of N‐(Mercaptomethyl)‐Phthalimide‐Carbonyl‐¹⁴C‐S‐(O,O‐Dimethylphosphorodithioate)

Leaffer

Skinner

Menn³

et al. 1967

J. Labelled Cpd. Radiopharm.

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N -(mercaptomethyl) -phthalimide-carbonyl-14C-S-(0,O- Dimethylphosphorodithioate) has been synthesized. The starting material was carboxyl labelled o-toluic acid which was oxidized to o-phthalic acid. Phthalimide (carbonyl-W) was prepared from o-pkthalic acid by subliming the ammonium salt of the acid. When 14C phthalimide was reacted with aqueous formaldehyde, N-hydroxymethyl phthalimide was formed. The final product was obtained when the N-hydroxymethyl derivative was reacted with thionyl chloride, followed by reaction with sodium dimethyl phosphorodithioate.

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¹³C, ¹³C coupling constants in anthracene, 9,10‐dihydroanthracene and phthalic acid derivatives. Determination of signs by the symmetrical double labelling (SDL) method V

Hansen

Berg

1979

Org. Magn. Reson.

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Synthesis of Anthracene-9-C ₁ ¹⁴

Cited by 4 publications

References 2 publications

Synthesis of ¹⁴C‐labeled flame retardants. ¹⁴C‐labeled‐tetrabromophthalic anhydride and tetrabromobisphenol‐A

Synthesis of ¹⁴C‐labeled flame retardants. ¹⁴C‐labeled‐tetrabromophthalic anhydride and tetrabromobisphenol‐A

Synthesis of N‐(Mercaptomethyl)‐Phthalimide‐Carbonyl‐¹⁴C‐S‐(O,O‐Dimethylphosphorodithioate)

¹³C, ¹³C coupling constants in anthracene, 9,10‐dihydroanthracene and phthalic acid derivatives. Determination of signs by the symmetrical double labelling (SDL) method V

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Synthesis of Anthracene-9-C 1 14

Cited by 4 publications

References 2 publications

Synthesis of 14C‐labeled flame retardants. 14C‐labeled‐tetrabromophthalic anhydride and tetrabromobisphenol‐A

Synthesis of 14C‐labeled flame retardants. 14C‐labeled‐tetrabromophthalic anhydride and tetrabromobisphenol‐A

Synthesis of N‐(Mercaptomethyl)‐Phthalimide‐Carbonyl‐14C‐S‐(O,O‐Dimethylphosphorodithioate)

13C, 13C coupling constants in anthracene, 9,10‐dihydroanthracene and phthalic acid derivatives. Determination of signs by the symmetrical double labelling (SDL) method V

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Product

Resources

About

Synthesis of Anthracene-9-C ₁ ¹⁴

Synthesis of ¹⁴C‐labeled flame retardants. ¹⁴C‐labeled‐tetrabromophthalic anhydride and tetrabromobisphenol‐A

Synthesis of ¹⁴C‐labeled flame retardants. ¹⁴C‐labeled‐tetrabromophthalic anhydride and tetrabromobisphenol‐A

Synthesis of N‐(Mercaptomethyl)‐Phthalimide‐Carbonyl‐¹⁴C‐S‐(O,O‐Dimethylphosphorodithioate)

¹³C, ¹³C coupling constants in anthracene, 9,10‐dihydroanthracene and phthalic acid derivatives. Determination of signs by the symmetrical double labelling (SDL) method V