1969
DOI: 10.1002/jlcr.2590050209
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Synthesis of kryptogenin‐26‐14C and diosgenin‐26‐14C

Abstract: SUMMARY Kryptogenin-26-I4C (13) was synthesized from dihydrodiosgenin diacetate (1). The radioactive carbon atom was introduced by the Arndt-Eistert method, and the extra carbon atom was then removed by a carboxy-inversion reaction. Diosgenin-26-I4C (14) was prepared by reduction of kryptogenir~-26-~~C.INTRODUCTION.

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