Synthesis of LiMn1/3Ni1/3Co1/3O2 in molten KCl for rechargeable lithium-ion batteries

Synthesis of LiNi1/3Co1/3Mn1/3O2 cathode materials by using a supercritical water method in a batch reactor

“…However, this preparation process causes inhomogeneity, irregular morphology, large particle size, and broad particle size distribution, and it requires long heating times followed by several grinding and annealing processes [11]. Various synthesis methods have been applied to overcome these drawbacks which include the combustion process [5,25,26], the co-precipitation method [23,27,30], molten salt synthesis [20], the sol-gel method [8,22], the spray dry method [2,10,28], and spray pyrolysis synthesis [11,19,29].…”

Effects of precipitator on the morphological, structural and electrochemical characteristics of Li[Ni1/3Co1/3Mn1/3]O2 prepared via carbonate coprecipitation

“…Many methods such as the solid state synthesis [11], the sol-gel method [12], the coprecipitation method [13,14], the molten salt method [15], etc., have been developed to prepared Li[Ni 1/3 Co 1/3 Mn 1/3 ]O 2 . Among these methods, coprecipitation has been widely adopted as the preferred method, because it allows for a better cationic distribution control and ease of handling [16,17].…”

Synthetic optimization of nanostructured Li[Ni1/3Mn1/3Co1/3]O2 cathode material prepared by hydroxide coprecipitation at 273K

“…Many methods such as the solid state synthesis [8], the sol-gel method [9], the combustion method [10], the coprecipitation method [11], the molten salt method [12], etc., have been developed to prepared high quality Li[Ni 1/3 Co 1/3 Mn 1/3 ]O 2 . Among these methods, coprecipitation has been widely adopted as the preferred method to produce mixed transition-metal hydroxide precursors with good cationic distribution.…”