Abstract.The method for identification of the triplet of kinetic parameters of a heterogeneous reaction using the data of the derivatographic analysis is proposed. This method is characterized by high accuracy and relative simplicity and it can be effectively realized using MS Excel software.Metal nanopowder is one of the most prospective high-energy materials that is widely used in many spheres [1,2]. This explains long and sustained interest in studying the features of metal nanopowder, in particular the kinetics of oxidation [3]. The proceeding heterogeneous reaction can be in full measure characterized by the so-called "kinetic triplet" -the frequency factor A, the activation energy and the mathematical description of the reaction mechanism f(α) [4,5,6].To identify these three parameters, the data of the derivatographic experiment conducted in the non-isothermal mode are used, when the change in the degree of transformation of the material α over time t is described by the differential equationUnder the temperature-linear heating where the rate of temperature increase T with a given parameter β = ⁄ and a specific mechanism (α) = (1 − α) , the kinetic equation (1) can be represented aswhere n -order (index) of reaction. Equation (2) has no analytical solution and numerical methods or approximate analytical ones are used to determine the kinetic parameters.The aim of this paper is to represent a quantitative result analysis of the derivatographic study of oxidation on the basis of a new approach to calculating the kinetic parameters of a Corresponding author: bvborisov@tpu.ru