Synthesis of nano B2O3/TiO2 composite material as a new solid phase extractor and its application to preconcentration and separation of cadmium

Kalfa, Orhan Murat; Yalcinkaya, Ozcan; Türker, Ali Rehber

doi:10.1016/j.jhazmat.2008.11.112

Cited by 154 publications

(66 citation statements)

References 31 publications

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“…18,19 TiO 2 NPs have been tested as a sorbent in the solid-phase extraction for preconcentrated lead (Pb) in river water and seawater. [20][21][22] Zhang et al 20 investigated the potential acute toxicity of the interaction between TiO 2 NPs (50 nm and 120 nm) and lead acetate (PbAC) in mice. Suspensions of TiO 2 NPs (5 g/kg body weight) alone, PbAC (500 mg/kg) alone, and TiO 2 NPs (5 g/kg) plus PbAC (500 mg/kg) were administered to mice via oral gavage, respectively.…”

Section: Effects Of Tio 2 Np Interaction With Metals and Their Compoundsmentioning

confidence: 99%

Toxic effects of the interaction of titanium dioxide nanoparticles with chemicals or physical factors

Liu

Lin²,

Zhao

2013

IJN

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Due to their chemical stability and nonallergic, nonirritant, and ultraviolet protective properties, titanium dioxide (TiO 2 ) nanoparticles (NPs) have been widely used in industries such as electronics, optics, and material sciences, as well as architecture, medicine, and pharmacology. However, increasing concerns have been raised in regards to its ecotoxicity and toxicity on the aquatic environment as well as to humans. Although insights have been gained into the effects of TiO 2 NPs on susceptible biological systems, there is still much ground to be covered, particularly in respect of our knowledge of the effects of the interaction of TiO 2 NPs with other chemicals or physical factors. Studies suggest that interactions of TiO 2 NPs with other chemicals or physical factors may result in an increase in toxicity or adverse effects. This review highlights recent progress in the study of the interactive effects of TiO 2 NPs with other chemicals or physical factors.

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Section: Effects Of Tio 2 Np Interaction With Metals and Their Compoundsmentioning

confidence: 99%

Toxic effects of the interaction of titanium dioxide nanoparticles with chemicals or physical factors

Liu

Lin²,

Zhao

2013

IJN

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“…The limits of detection of the proposed procedure for the determination of analyte elements were studied under the optimal experimental conditions. The detection limits, defined as the concentration equivalent to three times the standard deviation of blank divided to preconcentration factor (n = 10, X L = (X b + 3s)/PF, X L : Limit of Detection, X b : Blank Value, PF: preconcentration factor) (Kalfa et al 2009;Soylak et al 2010;He et al 2010) of the reagent blank were 1.6 μg L −1 for iron and 4.9 μg L −1 for lead.…”

Section: Analytical Performancementioning

confidence: 99%

Solid-phase extraction of heavy metal ions on bucky tubes disc in natural water and herbal plant samples

Soylak

Ünsal

2011

Environ Monit Assess

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A preconcentration-separation procedure has been established based on solid-phase extraction of Fe(III) and Pb(II) on bucky tubes (BTs) disc. Fe(III) and Pb(II) ions were quantitatively recovered at pH 6. The influences of the analytical parameters like sample volume, flow rates on the recoveries of analytes on BT disc were investigated. The effects of co-existing ions on the recoveries were also studied. The detection limits for iron and lead were found 1.6 and 4.9 μg L⁻¹, respectively. The validation of the presented method was checked by the analysis of TMDA-51.3 fortified water certified reference material. The presented procedure was successfully applied to the separation-preconcentration and determination of iron and lead content of some natural water and herbal plant samples from Kayseri, Turkey.

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“…where xblank is the mean concentration of the blank solution, sblank is the standard deviation of the blank solution, and PF is the preconcentration factor [49,50]. The detection limit for nickel(II) (N = 10) was 4.87 lg/L.…”

Section: Detection Limitmentioning

confidence: 99%

Membrane Filtration of Nickel(II) on Cellulose Acetate Filters for Its Preconcentration, Separation, and Flame Atomic Absorption Spectrometric Determination

Soylak¹,

Ünsal

Aydın

et al. 2010

CLEAN Soil Air Water

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An enrichment method for trace amounts of Ni(II), as 8-hydroxyquinoline chelates, has been established on a cellulose acetate membrane filter. Ni(II)-8-hydroxyquinoline chelates adsorbed on a membrane filter were eluted using 5 mL of 1 M HNO 3 . The eluent nickel concentration was determined by a flame atomic absorption spectrometer. The influence of some analytical parameters, including pH, amount of reagent, sample volume, etc., on recovery was investigated. The interference of co-existent ions was studied. The nickel detection limit was 4.87 lg/L. The method was applied to real samples for the determination of nickel(II) ions.

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Synthesis of nano B2O3/TiO2 composite material as a new solid phase extractor and its application to preconcentration and separation of cadmium

Cited by 154 publications

References 31 publications

Toxic effects of the interaction of titanium dioxide nanoparticles with chemicals or physical factors

Toxic effects of the interaction of titanium dioxide nanoparticles with chemicals or physical factors

Solid-phase extraction of heavy metal ions on bucky tubes disc in natural water and herbal plant samples

Membrane Filtration of Nickel(II) on Cellulose Acetate Filters for Its Preconcentration, Separation, and Flame Atomic Absorption Spectrometric Determination

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