Synthesis of pyridothietone by flash vacuum pyrolysis of 2-mercaptonicotinic acid

Chou, Chin-Hsing; Chiu, Shao-Jung; Liu, Weimin

doi:10.1016/s0040-4039(02)01044-4

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Formation From 3-hydroxy Thiol Derivatives1

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2008

2023

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Cited by 9 publications

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“…Such thermal formation of thietanes was shown to be possible when benzotriazoles [247] or acids [248] were present as reaction groups instead of alcohol functions (Scheme 3.138). Thietan-2-ones are formed by the reaction of 3-mercaptocarboxylic acids with DCC [249], i butyl chloroformate [250], methyl chloroformate [251], Ac 2 O [252], diethyl cyanophosphonate [253] or 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride (EDAC) (Scheme 3.139) [254].…”

Section: Formation From 3-hydroxy Thiol Derivativesmentioning

confidence: 99%