Synthesis of (Tetrazole, Oxazepine, Azo, Imine) Ligands and Studying of Their (Organic Identification, Chromatography, Solubility, Physical, Thermal Analysis, Bio-Study)

Alfatlawi, Intisar Obaid; Sahab, Eman Hassan; Aljamali, Nagham Mahmood

doi:10.5958/0974-360x.2018.00521.8

Cited by 6 publications

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“…Six protons appeared as a triplet at  0.93-0.95 which could be assigned to -CH3, protons appeared as a multiple at  1.6-1.9 ppm which could be assigned to (-CH2-)6 (24 H). The -OCH2 groups of pentyl substituent appeared as a triplet at  3.80-3.83 ppm (Alfatlawi et al, 2018). As seen in Figure 9, the EDX mapping of compounds D1-D3 including additives reveals the distribution and relative abundance of atoms within the mixes.…”

Section: Resultsmentioning

confidence: 92%

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Synthesis and characterization of new 1,3-Oxazepine-4,7-dione compounds from 1,2-diaminobenzene

Jebur¹,

Albdere

Al-Hussainawy³

et al. 2022

ijhs

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In this research, done synthesized a series of new 1,3-oxazepine-4,7-dione derivatives as D1-D3 compounds via using [2+5] cycloaddition reaction. Synthesized compounds that have been bis azo groups [B1-B3] from 1,2-diaminobenzene via coupling its diazonium salt with phenoxide anion of 4-alkoxybenzaldehyde which Alkoxy was as pentyl, hexyl, and Heptyl groups. These compounds B1-B3 are condensed with 4-Bromoaniline in Schiff bases reactions to give bisazoimine derivatives C1-C3. The compounds C1-C3 were produced by cycloaddition reaction to produce 1,3-oxazepine-4,7-dione derivatives D1-D3. The structures of the synthesized compounds are characterized by spectroscopic methods, such as FTIR, and 1HNMR spectra with the elemental composition analysis. The compounds D1-D3 that are synthesized play a big role in the inhibition of growth.

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Section: Resultsmentioning

confidence: 92%

“…General procedure for the synthesis of Oxazepine compounds (D1-D3)(Alfatlawi et al, 2018;Ayfan et al, 2019) …”

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confidence: 99%