Synthesis of the branched tetrasaccharide fragment of saccharomicin B

Garreffi, Brian P; Maney, Akash P.; Bennett, Clay S.

doi:10.1016/j.tetlet.2023.154615

Tetrahedron Letters

2023

DOI: 10.1016/j.tetlet.2023.154615

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Synthesis of the branched tetrasaccharide fragment of saccharomicin B

Brian P Garreffi

Akash P. Maney

Clay S. Bennett

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2024

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Cited by 1 publication

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Gram-Scale Synthesis of the Fucose-Containing Fragments of Saccharomicins

Fu,

Li,

et al. 2024

Org. Lett.

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A highly efficient synthetic route has been established for the gram-scale production of fucose−aglycon (Fuc−Agl) and fucose−saccharosamine (Fuc−Sac) fragments in saccharomicins A and B. The β-glycosidic bonds within these structural components were formed through successive rhodium(II) and Brønsted-acid-catalyzed glycosylation, utilizing a stable thioglycosyl donor. Subsequent steps involving the installation of protecting groups yielded highly functionalized synthetic fragments that are suitable for further assembly of saccharomicins.

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Gram-Scale Synthesis of the Fucose-Containing Fragments of Saccharomicins

Fu,

Li,

et al. 2024

Org. Lett.

View full text Add to dashboard Cite

show abstract

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Synthesis of the branched tetrasaccharide fragment of saccharomicin B

Cited by 1 publication

References 23 publications

Gram-Scale Synthesis of the Fucose-Containing Fragments of Saccharomicins

Gram-Scale Synthesis of the Fucose-Containing Fragments of Saccharomicins

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