The review delves into a rich tapestry of methodologies, spanning from the utilization of metals to the manipulation of light, and from electrochemical pathways to additive‐free approaches. Its aim is to meticulously compile and elucidate these diverse pathways, providing comprehensive insights into the strategies and methodologies utilized for synthesizing these compounds. By undertaking this exploration, its goal is to shed light on the intricate techniques employed in this field, consequently driving notable progress across disciplines ranging from biochemistry to medicinal research.