Synthesis, structural, electrical and optical properties of LiPr(PO3)4

Gharouel, S.; Smida, Youssef Ben; Ferhi, M.; Marín, Josefa Isasi; Alcaraz, Lorena; Cid, Pablo Arévalo; Horchani−Naifer, Karima; Férid, Mokhtar

doi:10.1016/j.jssc.2020.121459

Cited by 5 publications

(3 citation statements)

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“…Usually, the flux method is used to grow materials as single crystals [40]. The main objective of this method is to decrease the crystallization temperature.…”

Section: Flux Methodsmentioning

confidence: 99%

“…For more clarification, taking the example of LiPr(PO 3 ) 4 [40]. The material has been synthesized as a single crystal by the means of flux method.…”

Section: Flux Methodsmentioning

confidence: 99%

“…Finally, the mixture was cooled slowly to room temperature. The single crystal was separated from the excess phosphoric acid by washing in boiling water [40].…”

Section: Flux Methodsmentioning

confidence: 99%

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Synthesis Methods in Solid-State Chemistry

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Synthesis Methods and Crystallization

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The synthesis of single crystal is an area of intense activity in the materials science. The obtaining of the single crystal with sufficient dimension for X-ray diffraction depends on several factors including the chemical composition, crystal structure of the reagents, and physical parameters (temperature and pressure). In this context, this chapter is dedicated to the description of the most common synthesis methods of single crystal in the solid-state chemistry: solid-state method, hydrothermal, and slow evaporation at room temperature. Same other materials can be obtained at high pressure. There are also some physical techniques to grow single crystal, each technique is specific for specific materials.

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“…Usually, the flux method is used to grow materials as single crystals [40]. The main objective of this method is to decrease the crystallization temperature.…”

Section: Flux Methodsmentioning

confidence: 99%

“…For more clarification, taking the example of LiPr(PO 3 ) 4 [40]. The material has been synthesized as a single crystal by the means of flux method.…”

Section: Flux Methodsmentioning

confidence: 99%