2016
DOI: 10.1016/j.inoche.2015.12.010
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Synthesis, structures and properties of a meso -substituted pyrazolyl porphyrin and its Co(II) porphyrin complex

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Cited by 14 publications
(6 citation statements)
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“…Pyridine was distilled prior to use also (bp 115.2 °C). (2,3,7,8,12,18-Hexamethyl-13,17-diethyl-5-(2-pyridyl) porphyrin was synthesized by reaction of 2,2′-methylene-bis(3-ethyl-4-methyl-1H-pyrrole) with 3,4-dimethyl-1H-pyrrole-2-carbaldehyde in butan-1-ol in the presence of hydrobromic acid at room temperature followed by boiling with pyridine-2-carbaldehyde. [13] The UV-Visible spectra were measured on Agilent 8453 UVVisible spectrophotometers.…”
Section: Methodsmentioning
confidence: 99%
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“…Pyridine was distilled prior to use also (bp 115.2 °C). (2,3,7,8,12,18-Hexamethyl-13,17-diethyl-5-(2-pyridyl) porphyrin was synthesized by reaction of 2,2′-methylene-bis(3-ethyl-4-methyl-1H-pyrrole) with 3,4-dimethyl-1H-pyrrole-2-carbaldehyde in butan-1-ol in the presence of hydrobromic acid at room temperature followed by boiling with pyridine-2-carbaldehyde. [13] The UV-Visible spectra were measured on Agilent 8453 UVVisible spectrophotometers.…”
Section: Methodsmentioning
confidence: 99%
“…Co(AcO) 2 ⋅4H 2 O (47.0 mg, 0.19 mmol) and (2,3,7,8,12,18-hexamethyl-13,17-diethyl-5-(2-pyridyl)porphyrin H 2 P (20.0 mg, 0.04 mmol) were reacted in boiling dimethylformamide (10 ml) for 20-30 min. Completion of the reaction was monitored by TLC, until no traces of starting material were detected.…”
Section: Methodsmentioning
confidence: 99%
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