“…This led to several meetings (Lytle et al, 1989), a workshop and a report (Sayers, 2000a,b) over a similar time period, however, without a resulting laboratory or synchrotron benchmark or round-robin. XAFS began with local sources (Fricke, 1920;Lytle, 1965Lytle, , 1966Lytle et al, 1975), but it was soon understood that synchrotron sources dominated for the acquisition of high-flux high-precision data sets (Lapeyre et al, 1983;Doniach et al, 1997;Lynch, 1997). Indirectly, this initiative has led to the development of some standard practices at synchrotron beamlines for sample preparation and data collection (Newville, 2004;Bunker, 2010).…”