a b s t r a c tThe effects of post-annealing temperature were investigated on Bi 2 Sr 2 Ca 1 Cu 2 O 8+o thin films deposited on MgO (1 0 0) substrates by pulsed laser deposition (PLD). The structural and superconducting properties of the films have been determined by means of X-ray diffraction (XRD), scanning electron microscopy (SEM), temperature depende nt resistivity (R-T), and DC magnetization measure ments. The films which were deposited at 600 °C were post-annealed in an atmosphere of a gas mixture of Ar (93%) and O 2 (7%), at temperature ranging between 800 and 880 °C. This resulted in films which exhibited a single phase of 2212 with a high crystallini ty (FWHM % 0.16°) and texturing along the c-axis, perpendicular to the plane of the substrate. An optimum temperature of 860 °C was found for the post-annealing thermal treatment. The critical temperature, T C , of the films was measure d as 82 K and the critical current density, J C , was calcu lated as 3 Â 10 7 A/cm 2 for the film annealed at 860 °C.