In this paper, the problem of creating homogeneous composites with on carbon nanotubes is described. To control the quality of the manufactured composites, a system of terahertz visualization of material inhomogeneity using a continuous radiation source is used. An increase in the homogeneity of the composite based on multi-walled carbon nanotubes with an increase in the time of ultrasonic processing during polymerization is noted. The advantages of THz imaging in comparison with optical microscopy are shown.