We describe the development of a novel instrument intended for the measurement of the acoustical reflection coefficient of materials. The instrument effectively implements a one-port vector-corrected network analyzer in the acoustic, rather than the electromagnetic, domain. Employing the welldocumented methods of error correction familiar to microwave engineers, this instrument permits automated measurement of an acoustic impedance presented to a waveguide port. A dualdirectional coupler allows a working frequency range of well over an octave. In principle, a set of six couplers would allow measurement from 100 to 50 000 Hz.