The crystal structure of hexakis(1-ethylimidazole-κ1
 N)nickel(II) dichloride – 1-ethylimidazole (1/2), C40H64Cl2NiN16

He, Qingpeng; Liu, Sen; Xue, Zheng

doi:10.1515/ncrs-2021-0113

Zeitschrift Für Kristallographie - New Crystal Structures

2021

DOI: 10.1515/ncrs-2021-0113

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The crystal structure of hexakis(1-ethylimidazole-κ¹ N)nickel(II) dichloride – 1-ethylimidazole (1/2), C₄₀H₆₄Cl₂NiN₁₆

Qingpeng He

Sen Liu

Zheng Xue

Abstract: C40H64Cl2NiN16, monoclinic, P21/c (no. 14), a = 8.2320(9) Å, b = 16.2902(16) Å, c = 17.3843(17) Å, α = 90°, β = 101.773(3)°, γ = 90°, V = 2282.2(4) Å3, Z = 2, R gt (F) = 0.0448, wR ref (F 2) = 0.1181, T = 298(2) K.

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Synthesis, characterization, and crystal structure of hexakis(1-methyl-1H-imidazole-κN ³)zinc(II) dinitrate

Magwa,

Rashamuse

2024

Acta Crystallogr E Cryst Commun

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The synthesis of the title compound, [Zn(C4H6N2)6](NO3)2, is described. This complex consists of a central zinc metal ion surrounded by six 1-methylimidazole ligands, charge balanced by two nitrate anions. The complex crystallizes in the space group P\overline{3}. In the crystal, the nitrate ions are situated within the cavities created by the [Zn(N-Melm)6]2+ cations, serving as counter-ions. The three oxygen atoms of the nitrate ion engage in weak C—H...O interactions. In addition to single-crystal X-ray diffraction analysis, the complex was characterized using elemental analysis, 1H NMR, 13C NMR, and FTIR spectroscopy.

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Synthesis, characterization, and crystal structure of hexakis(1-methyl-1H-imidazole-κN ³)zinc(II) dinitrate

Magwa,

Rashamuse

2024

Acta Crystallogr E Cryst Commun

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The crystal structure of hexakis(1-ethylimidazole-κ¹ N)nickel(II) dichloride – 1-ethylimidazole (1/2), C₄₀H₆₄Cl₂NiN₁₆

Abstract: C40H64Cl2NiN16, monoclinic, P21/c (no. 14), a = 8.2320(9) Å, b = 16.2902(16) Å, c = 17.3843(17) Å, α = 90°, β = 101.773(3)°, γ = 90°, V = 2282.2(4) Å3, Z = 2, R gt (F) = 0.0448, wR ref (F 2) = 0.1181, T = 298(2) K.

Cited by 1 publication

References 10 publications

Synthesis, characterization, and crystal structure of hexakis(1-methyl-1H-imidazole-κN ³)zinc(II) dinitrate

Synthesis, characterization, and crystal structure of hexakis(1-methyl-1H-imidazole-κN ³)zinc(II) dinitrate

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The crystal structure of hexakis(1-ethylimidazole-κ1 N)nickel(II) dichloride – 1-ethylimidazole (1/2), C40H64Cl2NiN16

Abstract: C40H64Cl2NiN16, monoclinic, P21/c (no. 14), a = 8.2320(9) Å, b = 16.2902(16) Å, c = 17.3843(17) Å, α = 90°, β = 101.773(3)°, γ = 90°, V = 2282.2(4) Å3, Z = 2, R gt (F) = 0.0448, wR ref (F 2) = 0.1181, T = 298(2) K.

Cited by 1 publication

References 10 publications

Synthesis, characterization, and crystal structure of hexakis(1-methyl-1H-imidazole-κN 3)zinc(II) dinitrate

Synthesis, characterization, and crystal structure of hexakis(1-methyl-1H-imidazole-κN 3)zinc(II) dinitrate

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The crystal structure of hexakis(1-ethylimidazole-κ¹ N)nickel(II) dichloride – 1-ethylimidazole (1/2), C₄₀H₆₄Cl₂NiN₁₆

Synthesis, characterization, and crystal structure of hexakis(1-methyl-1H-imidazole-κN ³)zinc(II) dinitrate

Synthesis, characterization, and crystal structure of hexakis(1-methyl-1H-imidazole-κN ³)zinc(II) dinitrate