Supersonic jet exhaust plumes produce noise in jet engines, which has been a problem in the aerospace field. Researchers are working on ways to reduce this turbulent mixing noise, with little modification to the engine and nozzle. Prior work has shown that total temperature non-uniformity is a noise reduction technique which introduces a stream of cold flow into the heated jet. This method has been shown to cause changes in the exhaust plume and result in a 2±0.5 dB reduction of peak sound pressure levels. The goal of this work is to reveal underlying changes in the spatial-temporal structure of plume instability and turbulence caused by non-uniform total temperature distributions. Studies have demonstrated several methods of jet noise reduction by modifying the turbulent mixing in the exhaust plume. Large-scale turbulent structures have been shown to be the dominant source of noise in heated supersonic jets, especially over long, streamwise distances. Therefore, a large field-of-view measurement is desirable for studying these structures. Time-Resolved Doppler Global Velocimetry (TR-DGV) with a sampling frequency of 50 kHz is used to collect flow velocity data that is resolved in both time and space.The experiments for data collection were performed on a heated supersonic jet at the Virginia Tech Advanced Propulsion and Power Laboratory. A converging-diverging nozzle with a diameter Reynolds number of 850,000 was used to generate a perfectly expanded, heated flow of Mach 1.5 and a nozzle pressure ratio (NPR) of 3.67. The unheated plume was introduced at the center of the nozzle, with a total temperature ratio (TTR) of 2. Comparison of the mean velocity fields shows that the introduction of the cooler temperature flow in the thermally non-uniform case results in a velocity deficit of about 10% compared to the thermally uniform case. The method of spectral proper orthogonal decomposition (SPOD) was used to reveal the large-scale, coherent noise producing mechanisms. SPOD results indicate that the thermally non-uniform case showed a decrease in turbulent kinetic energy compared to the uniform case at all frequencies. Coherent fluctuations start developing further upstream in the thermally non-uniform case. The addition of the unheated plume results in a disruption in the propagation of the Mach waves from the shear layer into the ambient. The results indicate that the total temperature nonuniformity results in a modified exhaust plume and mean flow distribution at the nozzle exit, compared to that of a thermally uniform flow, which past studies have indicated is a method to reduce jet noise.I would like to thank my advisor, Dr. Todd Lowe, for his support, encouragement, and patience throughout these past two years. There were times when I felt discouraged when struggling to balance my research, graduate school courses, and a full-time job, but you had faith in me and pushed me to achieve my goals. To my co-chair, Dr. Wing Ng, thank you for your constant feedback throughout the duration of my master's degree. Comple...