The Detection of Heavy Metals from Biological Material by GLC and HPLC via the Diethyldithiocarbamates (DEDTC)

Drasch, G.; Kauert, G.; Meyer, Lina

doi:10.1515/9783112417225-099

Proceedings of the Second International Workshop Neuherberg, Federal Republic of Germany, April 1982 1983

DOI: 10.1515/9783112417225-099

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The Detection of Heavy Metals from Biological Material by GLC and HPLC via the Diethyldithiocarbamates (DEDTC)

G. Drasch¹,

G. Kauert²,

Lina Meyer³

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1985

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Determination of Pd and Co as Their Dithiocarbamate Complexes by Liquid Chromatography without Solvent Extraction

Mueller

Lovett

1985

Analytical Letters

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High performance reverse-phase liquid chromatography with UV-detection can be used to determine race levels of Pd and C o a s their dithiocarbamate complexes by direct injection of aqueous acetonitrile solutions of the metal containing dithiocarbamate. An excess of ligand, a t least f o u r times that required to form the neutral metal complex, was necessary for complete metalcomplex formation. T h e presence of other metal species and the solution acidity depleted the amount o f ligand available € o r complexation. Detection limits for Pd(I1) and Co(1II) from aqueous solution a s their dithiocarbamate complexes were 2.7 ng/mL and 9.5 n g / m L respectively. Trace le'vels of Pd i n 2399 MUELLER AND LOVETTp l a t i n u m p o w d e r ( 6 2 u g / g ) h a v e b e e n d e t e r m i n e d .

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Determination of Pd and Co as Their Dithiocarbamate Complexes by Liquid Chromatography without Solvent Extraction

Mueller

Lovett

1985

Analytical Letters

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show abstract

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The Detection of Heavy Metals from Biological Material by GLC and HPLC via the Diethyldithiocarbamates (DEDTC)

Cited by 1 publication

References 0 publications

Determination of Pd and Co as Their Dithiocarbamate Complexes by Liquid Chromatography without Solvent Extraction

Determination of Pd and Co as Their Dithiocarbamate Complexes by Liquid Chromatography without Solvent Extraction

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