The development of combinatorial chemistry methods for coating development

Chisholm, Bret J.; Potyrailo, Radislav A.; Cawse, James N.; Shaffer, Ronald E.; Brennan, Michael J.; Molaison, Chris; Whisenhunt, Donald W.; Flanagan, Bill; Olson, Dan; Akhave, Jay; Saunders, Dennis; Mehrabi, Ali Reza; Licon, Mark

doi:10.1016/s0300-9440(02)00115-7

Cited by 61 publications

(36 citation statements)

References 7 publications

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“…The concept satisfies the essential needs of high data compatibility and versatility together with convenient data import and export. Potyrailo and co-workers [121][122][123] presented a centralized data-management and storage system for their work on organic polymer and hybrid coatings. One important fact of their approach is the sharing of information from synthesis, testing, and evaluation by the database.…”

Section: Reviewsmentioning

confidence: 99%

Combinatorial and High‐Throughput Materials Science

2007

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There is increasing acceptance of high-throughput technologies for the discovery, development, and optimization of materials and catalysts in industry. Over the years, the relative synchronous development of technologies for parallel synthesis and characterization has been accompanied by developments in associated software and information technologies. This Review aims to provide a comprehensive overview on the state of the art of the field by selected examples. Technologies developed to aid research on complex materials are covered as well as databases, design of experiment, data-mining technologies, modeling approaches, and evolutionary strategies for development. Different methods for parallel synthesis provide single sample libraries, gradient libraries for electronic or optical materials, similar to polymers and catalysts, and products produced through formulation strategies. Many examples illustrate the variety of isolated solutions and document the barely recognized variety of new methods for the synthesis and analysis of almost any material. The Review ends with a summary of success stories and statements on still-present problems and future tasks.

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Section: Reviewsmentioning

confidence: 99%

Combinatorial and High‐Throughput Materials Science

2007

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“…Indeed, one major challenge in this field is the efficient exploration of this large parameter space in order to develop an understanding of the fundamental driving forces for development of adhesive strength at polymer/polymer, polymer/metal, polymer/ceramic, and polymer/biomaterial interfaces. The ability to conduct highly parallel tests and employ multivariant libraries is an essential step toward rapidly and efficiently identifying structure-property relationships critical for tuning adhesive performance [81,82]. At NIST, we developed several combinatorial and high-throughput measurement platforms for probing both the fundamental origins of adhesion (e.g., interfacial interactions) as well as practical aspects of adhesion in soft materials (e.g., PSAs) as well as glassy materials and thermosets (e.g., epoxies).…”

Section: Adhesion Testingmentioning

confidence: 99%

“…Combinatorial and high-throughput measurements of adhesion in rigid coatings and films demand quite different approaches than soft adhesives such as PSAs [81,87,88]. For example, contact methods such as the probe tack test are not suitable for measuring the interfacial strength of a coating adhered to a substrate.…”

Section: Glassy Materials: Edge-delamination Testsmentioning

confidence: 99%

Gradient and Microfluidic Library Approaches to Polymer Interfaces

Fasolka¹,

Stafford²,

Beers³

2009

Polymer Libraries

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We present an overview of research conducted at the National Institute of Standards and Technology aimed at developing and applying combinatorial and high-throughput measurement approaches to polymer surfaces, interfaces and thin films. Topics include (1) the generation of continuous gradient techniques for fabricating combinatorial libraries of film thickness, temperature, surface chemistry and polymer blend composition, (2) high-throughput measurement techniques for assessing the mechanical properties and adhesion of surfaces, interfaces and films, and (3) microfluidic approaches to synthesizing and analyzing libraries of interfaciallyactive polymer species.

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“…These have included deposition into vials or wells of a multiwell plate, deposition using ink-jet printing, [57][58][59][60] microcontact printing, [61][62][63] deposition into wells formed by a removable template, [64][65][66] and the use of an automated draw-down system. [67][68][69][70] A challenge with all of these methods is to generate a film that is uniform in thickness and composition over the spatial area needed for property determination.…”

Section: Preparation Of Discrete Polymer Materials Librariesmentioning

confidence: 99%

Combinatorial and High‐Throughput Methods in Macromolecular Materials Research and Development

Webster

2008

Macro Chemistry & Physics

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Combinatorial and high‐throughput experimentation is used to accelerate the rate of experimentation in macromolecular science. Combinatorial and high‐throughput methods are used in macromolecular science to discover and optimize catalysts for polymerization reactions, discover compositions that have specific desired properties, and systematically explore polymer structure–property relationships. The use of high‐throughput methods can enable the discovery of complex catalyst systems or polymer compositions that would not be feasible using conventional experimental methods. In addition, combinatorial data can be used as inputs into computer models to enable the accurate prediction of material properties as a function of composition.magnified image

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The development of combinatorial chemistry methods for coating development

Cited by 61 publications

References 7 publications

Combinatorial and High‐Throughput Materials Science

Combinatorial and High‐Throughput Materials Science

Gradient and Microfluidic Library Approaches to Polymer Interfaces

Combinatorial and High‐Throughput Methods in Macromolecular Materials Research and Development

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