Abstract:In this paper, low-temperature solid-state processes of the dehydrogenation of ammonia borane (NH 3 BH 3 , AB) samples of different purity are compared under the conditions of isothermal heating at 100 • C, as well as in the course of thermal analysis which was also carried out at different rates of heating. The composition of boron-containing impurities was studied by attenuated total reflection Fourier transform infrared spectroscopy (ATR FTIR) and 11 B magic angle spinning nuclear magnetic resonance ( 11 B … Show more
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