2012
DOI: 10.1016/j.proeng.2012.02.047
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The Effect of Ultrasonic Treatment on the Particle Size and Specific Surface Area of LaCoO3

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Cited by 38 publications
(23 citation statements)
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“…Carabalí et al [33] synthesized LaCoO 3 by the acrylamide polymerization method using radiation, reporting that the compound begins its formation at 500 ∘ C and the formation of the single phase was around 700 ∘ C. Jung and Hong [24] reported the formation of LaCoO 3 at 650 ∘ C when it was prepared from an aqueous solution of metallic nitrate salts in presence of malic acid, later a drying process by microwave radiation, and finally a thermal treatment. Similarly, Sompech et al [34] synthesized perovskite at 600 ∘ C employing a mechanochemical method. In the present work, LaCoO 3 powders were obtained employing a microwave-assisted colloidal method in presence of ethylenediamine and a further calcination process from a temperature of 500 ∘ C and higher.…”
Section: Resultsmentioning
confidence: 99%
“…Carabalí et al [33] synthesized LaCoO 3 by the acrylamide polymerization method using radiation, reporting that the compound begins its formation at 500 ∘ C and the formation of the single phase was around 700 ∘ C. Jung and Hong [24] reported the formation of LaCoO 3 at 650 ∘ C when it was prepared from an aqueous solution of metallic nitrate salts in presence of malic acid, later a drying process by microwave radiation, and finally a thermal treatment. Similarly, Sompech et al [34] synthesized perovskite at 600 ∘ C employing a mechanochemical method. In the present work, LaCoO 3 powders were obtained employing a microwave-assisted colloidal method in presence of ethylenediamine and a further calcination process from a temperature of 500 ∘ C and higher.…”
Section: Resultsmentioning
confidence: 99%
“…By only 1 hour of the ball-milling, the particle size sharply decreased to ~18% of that of the untreated powder, and then size decreased to ~0.6μm after 4 hours. As generally well known, when the particle size decreased continuously, the surface area increased in contrast 17,18) . Also, Table 1 shows values of the mean particle size and the surface area for the untreated and the ball-milled LaCoO3 powders.…”
Section: Methodsmentioning
confidence: 70%
“…The fiber lengths of cellulose were reduced to 30-50 μm from the original value of 80-120 μm with 1 hr ultrasonication and became 20-30 μm with 5 hr treatment (Sumari et al, 2013). Similarly, the particle size of LaCoO 3 powders was decreased from 4.90 to 3.24, 2.89, and 1.74 µm after treating with ultrasonic bath for 2, 4, and 6 min, respectively (Sompech et al, 2012).…”
Section: Particle Size Distributionmentioning
confidence: 90%
“…(Santos et al, 2009). This cavitation effect of ultrasound could be used for reducing the particle size of organic substances (Bi et al, 2015;Gilca et al, 2015;Sumari et al, 2013) or inorganic substances (Franco et al, 2004;Hassan et al, 2013;Sompech et al, 2012).…”
mentioning
confidence: 99%