2011
DOI: 10.5618/chem.2011.v1.n1.4
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The First Inexpensive, Simplified and Large Scale Synthesis of p-tert-butylcalix[7] and [9]arenes

Abstract: The nuclear industry and the rare earth elements mining need methods in order to separate lanthanides and actinides. Large organic macrocycles have demonstrated their contribution to this domain. Due to the lack of an efficient and reproducible method of synthesis, the chemistry of large p-tert-butylcalix[n] arenes (with 6 < n < 10) has been much less explored than the one of their inferior homologs. Excepted for the p-tert-butylcalix[8]arene which is obtained in good yields, the procedures described in the li… Show more

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