The article explores the morphological and electrochemical properties of carbon electrode materials derived from D-lactose by mixing the carbon precursor with an activating reagent selected from the series KOH, K2CO3, ZnCl2, SnCl2 2H2O and calcining the composite mixture at 800 °. After dissolution and removal of K2O, ZnO or SnO from volume of prototypes, the specific surface of carbon materials increases 1.7-4.2 times, and the electrical conductivity-1.4-2.8 times. The activating reagents for effective influence on the properties of carbon structures can be placed in the following order: ZnCl2 > K > K2CO3 > SnCl2 2H2O. It is established that the highest specific capacity as an electrode material for supercapacitor has a sample with the highest electrical conductivity (78 hm-1 m-1) obtained using KOH activating reagent. The electrode material capacity was 176-157 F g-1 at discharge currents of 10-100 mA. It is found that the difference in the values of capacity of prototypes is caused by different chemical state of their surface.