The role of recrystallization and grain growth in optimizing the sheet texture of magnesium alloys with calcium addition during annealing

Guo, Fei; Pei, Risheng; Jiang, Luyao; Zhang, Dingfei; Korte‐Kerzel, Sandra; Al‐Samman, Talal

doi:10.1016/j.jma.2019.07.010

Cited by 50 publications

(14 citation statements)

References 51 publications

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“…Grain refinement is a well-known strengthening technique to enhance mechanical properties of the metallic materials. , Reinforcement particles in the MMC inhibit its grain growth during high temperature processing. The grain growth restriction is achieved by the pinning effect along the grain boundary, which further leads to the strengthening of the metal matrix. , Parande et al reported that incorporation of β-TCP in Mg matrix significantly reduced the grain size of the Mg/β-TCP and improved its mechanical properties. Similarly, β-TCP incorporation in the ZK60 alloy also exhibited grain refinement, and fine grains hindered the dislocation motion .…”

Section: Design Philosophy Of Composite Developmentmentioning

confidence: 99%

Recent Developments in Magnesium Metal–Matrix Composites for Biomedical Applications: A Review

Dutta

Gupta

Roy

2020

ACS Biomater. Sci. Eng.

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Recently, there is a growing interest in developing magnesium (Mg) based degradable biomaterial. Although corrosion is a concern for Mg, other physical properties, such as low density and Young’s modulus, combined with good biocompatibility, lead to significant research and development in this area. To address the issues of corrosion and low yield strength of pure Mg, several approaches have been adopted, such as, composite preparation with suitable bioactive reinforcements, alloying, or surface modifications. This review specifically focuses on recent developments in Mg-based metal matrix composites (MMCs) for biomedical applications. Much effort has gone into finding suitable bioactive, bioresorbable reinforcements and processing techniques that can improve upon existing materials. In summary, this review provides a comprehensive overview of existing Mg-based composite preparation and their mechanical and corrosion properties and biological responses and future perspectives on the development of Mg-based composite biomaterials.

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Section: Design Philosophy Of Composite Developmentmentioning

confidence: 99%

Recent Developments in Magnesium Metal–Matrix Composites for Biomedical Applications: A Review

Dutta

Gupta

Roy

2020

ACS Biomater. Sci. Eng.

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“…Multiple static recrystallizations clearly achieved refinement and homogenization of the structure during this process. Guo et al [31] studied the effects of recrystallization and grain growth during annealing in optimizing the texture of calcium-added magnesium alloy sheets and found that the recrystallized nucleus retained the orientation of its deformed matrix in AZ31, which provided limited potential for optimizing texture through annealing treatment. Therefore, it can be seen that the alloy can obtain good plasticity during the annealing process.…”

Section: Introductionmentioning

confidence: 99%

The Effect of Annealing on the Microstructure and Properties of Ultralow-Temperature Rolled Mg–2Y–0.6Nd–0.6Zr Alloy

Tan

et al. 2021

Metals

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Mg–2Y–0.6Nd–0.6Zr alloy was first deformed by equal channel angular pressing (ECAP), then rolled and deformed under ultralow temperature conditions (liquid nitrogen immersion), and finally annealed. Optical microscopy (OM), electron backscatter diffraction technology (EBSD), and transmission electron microscopy (TEM) were used to analyze the evolution of the multiscale microstructure and changes in the mechanical properties of the alloy under ultralow temperatures and various annealing conditions. The results showed that the alloy treated with ECAP obtained fine grains, and a large number of fine twins were formed during the ultralow-temperature rolling process, which promoted the improvement of its hardness and strength and provided numerous preferential nucleation sites. The annealing made it easier to induce recrystallization and improve the recrystallization nucleation rate. The twin boundary produced by the alloy after ultralow-temperature rolling and the uniform fine grains formed by annealing resulted in excellent strength and plasticity of the alloy. The twins formed after rolling under ultralow temperatures were mainly {1 0 1 2} <1011> tensile twins. The alloy had comprehensive mechanical properties with a tensile strength of 186.15 MPa and an elongation of 29% after annealing at 350 °C for 10 min.

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“…[16,17] Considering the differences in the pre-rolling regimes in their study and the present one (55 pct cold rolling vs 80 pct hot rolling), a furnace heat treatment at 350°C for a duration of 30 minutes seems to be rather reasonable to obtain a specimen in a partial recrystallization state. Compared with conventional Mg alloys such as AZ31, which readily recrystallizes within tens of seconds at 250°C and 300°C, [20,57] the retardation of the recrystallization kinetics due to the presence of Ce is more than evident.…”

Section: Nucleation Microstructurementioning

confidence: 97%

“…Therefore, the studies on texture modification through recrystallization during/after conventional rolling are far more frequent compared to asymmetric rolling, for example. [12][13][14][15][16][17][18][19][20] Mackenzie et al first reported an abnormal extrusion texture in a RE (RE = rare earths)-added alloy, WE43. Instead of orienting the basal planes approximately parallel to the extrusion direction, the recrystallized grains in the alloy were oriented with their basal planes at 45 deg to the extrusion axis.…”

Section: Introductionmentioning

confidence: 99%

“…[16,17] More recently, via similar rolling-annealing processing schemes, texture modification was also observed in RE-free sheets such as Mg-Zn-Ca, [24][25][26] Mg-Li-Ca, [27] Mg-Al-Ca, [28] and Mg-Al-Zn-Ca. [19,20] Aside from conventional furnace annealing, external field annealing has attracted considerable attention in the past few decades because it has been found to affect the recrystallization process of many ferromagnetic and non-ferromagnetic metallic materials. [29][30][31] Molodov et al have found that an applied magnetic field has a special influence on the annealing texture formation process of Zn, [32] Zr, [33] and Ti.…”

Section: Introductionmentioning

confidence: 99%

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On the Texture Weakening During Electropulse Annealing Treatment of Mg-1Ce Alloy: The Role of Nucleation and Nucleus Growth

Kuang

Al‐Samman

et al. 2020

Metall Mater Trans A

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Mg-1Ce alloys were pre-rolled at room temperature to various reductions to achieve different as-rolled microstructures. The deformed materials were then treated with a pulsed electric current (electropulse treatment, EPT) to study the effect of the as-rolled microstructure on the recrystallization texture formation. The experimental results show that an optimum window exists for pre-rolling reductions, within which the as-rolled microstructures and sharp basal textures obtained will evolve into fine recrystallized grains and weak textures during the subsequent EPT. Microstructure analysis indicates a competition between two processes, the nucleation and the nucleus growth, in contributing to the texture weakening of the alloy. While both the application of pulsed electric current and the increase in the pre-rolling reductions could strengthen the advantage of the nucleation rate of the non-basal nuclei over those with basal orientations, the contribution from nucleus growth depends mainly on the available deformed basal-oriented matrix, which decreases with increasing pre-rolling reductions. The results of the present study might provide useful guidance for the optimization of process parameters in the future application of the 'pre-rolling + EPT' technique on the Mg alloy sheet.

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The role of recrystallization and grain growth in optimizing the sheet texture of magnesium alloys with calcium addition during annealing

Cited by 50 publications

References 51 publications

Recent Developments in Magnesium Metal–Matrix Composites for Biomedical Applications: A Review

Recent Developments in Magnesium Metal–Matrix Composites for Biomedical Applications: A Review

The Effect of Annealing on the Microstructure and Properties of Ultralow-Temperature Rolled Mg–2Y–0.6Nd–0.6Zr Alloy

On the Texture Weakening During Electropulse Annealing Treatment of Mg-1Ce Alloy: The Role of Nucleation and Nucleus Growth

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