1954
DOI: 10.1021/ja01632a016
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The Synthesis of α-Alkoxy-β-haloethyl Acetates and 2-Aminothiazole

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Cited by 27 publications
(8 citation statements)
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“…During the course of our systematic study on application of N-halo compounds 24 in organic chemistry, we report, herein, our results on acetylation of a variety of alcohols with Ac 2 O using a catalytic amount of N,N-dichloro-4-methylbenzenesulphonimide (1), 25 under mild reaction conditions at room temperature (Scheme 1).…”
Section: Resultsmentioning
confidence: 99%
“…During the course of our systematic study on application of N-halo compounds 24 in organic chemistry, we report, herein, our results on acetylation of a variety of alcohols with Ac 2 O using a catalytic amount of N,N-dichloro-4-methylbenzenesulphonimide (1), 25 under mild reaction conditions at room temperature (Scheme 1).…”
Section: Resultsmentioning
confidence: 99%
“…The resulting precipitate of NNDBS was filtered, washed with water, and dried. A yellow solid was obtained (122.5 g) that melted at 114°C (lit., 115°C) (15).…”
Section: Methodsmentioning
confidence: 99%
“…[1][2][3] The methods that have been used extensively in oxidation of alcohol include the PCC catalyzed oxidation with periodic acid, 4 silica gel supported InBr 3 and InCl 3 5 , etc. [6][7][8][9][10][11][12][13] During the course of our systematic study on oxidation and halogenation of organic compounds with N-halo reagents, [14][15][16][17][18][19][20][21] we have found that N,N-dichloro-4-methylbenzenesulfonamide 22 is an inexpensive, easily obtained, moisture insensitive, low toxic and low corrosive reagent. We now report a convenient method for the oxidation of alcohols using N,N-dichloro-4-methylbenzenesulfonamide as oxidizing reagent, which overcomes the disadvantages associated with oxidative methods developed so far.…”
Section: Introductionmentioning
confidence: 99%