Though it has my name on it, this dissertation is the product of many people's hard work and dedication. First, I would like to thank my wife, Mackenzie DeRoo, who has sustained me both personally and professionally and has (somehow) always found interest in X-ray instrumentation. Through her consistent support of my 'need to work,' she is a co-author in absentia. I am grateful to my parents, who were my first co-investigators and copy editors, and who have always actively encouraged my academic pursuits. Next, my colleagues deserve a great deal of credit for their prodigious help. I'd like to thank Drew Miles, Ben Donovan, and Tom Peterson-they have been excellent students, even better teachers, and have enabled a great deal more of this work than I think they realize. I am grateful to Hannah Marlowe, my grating theory buddy, for sharing your knowledge of Python, L A T E X, and diffraction efficiency modeling. I'd like to thank Ted Schultz for his patience in instruction and willingness to impart engineering wisdom, as his advice on how to do something is rarely off the mark. I owe James Tutt the entirety of my knowledge of CCD detectors, and am grateful to him for his persistent willingness to help. His work ethic, loyalty, and dedication are professional characteristics I will strive to emulate in the future. Finally, I owe a great deal to my advisor, Randall McEntaffer. Obviously, he has enabled the subject matter of this work, which has made for an interesting graduate career ('Thanks, boss!'). More importantly, however, he has empowered me as a young scientist, bringing me from pupil to colleague long before I thought I was ready and, in so doing, made me one. Whether X-ray testing a new grating or singing Pitbull &