Thermal analysis of new dimethyl/dibutyl tin(IV) compounds with amino acids

Chilwal, Asha; Malhotra, Purnima; Narula, Anudeep Kumar

doi:10.1007/s10973-012-2880-7

Cited by 7 publications

(2 citation statements)

References 25 publications

Supporting

Mentioning

Contrasting

Order By: Relevance

“…The spectra of dimethyltin(IV) complexes exhibit two new medium‐intensity bands in the region 545 ± 5 and 615 ± 5 cm −1 which may be attributed to SnO bonds . The (SnC) sym and (SnC) asym stretching vibrations are observed in the regions 560 ± 5 and 600 ± 5 cm −1 , respectively . A strong band appears in the region 1570–1670 cm −1 in the spectra of fluorinated β‐diketone (L 1 H) and β‐diketones (L 2 H, L 3 H and L 4 H).…”

Section: Resultsmentioning

confidence: 97%

The structure–activity relationship of some hexacoordinated dimethyltin(IV) complexes of fluorinated β‐diketone/β‐diketones and sterically congested heterocyclic β‐diketones

Sharma

Jain

Saxena

2015

Applied Organom Chemis

View full text Add to dashboard Cite

The study was focused on the structure-activity relationship of some newly synthesized hexacoordinated dimethyltin(IV) complexes of fluorinated β-diketone/β-diketones and sterically congested heterocyclic β-diketones. These complexes were screened for their antibacterial activity against a Gram-negative bacterium (Pseudomonas aeruginosa) and Gram-positive bacteria (Streptomyces griseus, Staphylococcus aureus, Bacillus subtilis) and the results were compared with those of a standard antibacterial drug. Some of the complexes were also screened for their antifungal activity against various fungi (Aspergillus niger, A. flavus, Trichoderma viride, Fusarium oxysporum) and were found to be active. These new hexacoordinated complexes of dimethyltin (IV) were generated by reactions of dimethyltin(IV) dichloride and sodium salts of fluorinated β-diketone/β-diketones and sterically congested heterocyclic β-diketones in 1:1:1 molar ratio in refluxing dry benzene. Plausible structures of these complexes were suggested with the aid of physicochemical and spectroscopic studies. 119 Sn NMR spectral data revealed the presence of a hexacoordinated tin centre in these dimethyltin(IV) complexes.

show abstract

Section: Resultsmentioning

confidence: 97%

The structure–activity relationship of some hexacoordinated dimethyltin(IV) complexes of fluorinated β‐diketone/β‐diketones and sterically congested heterocyclic β‐diketones

Sharma

Jain

Saxena

2015

Applied Organom Chemis

View full text Add to dashboard Cite

show abstract

“…It is combined with other techniques, such as FTIR, NMR, and XRD [17][18][19][20][21][22][23]. The main concept of this work is to determine the thermal properties of three derivatives of 3,4-pyridinedicarboximides (slightly differ in molecular structure).…”

Section: Introductionmentioning

confidence: 99%

Synthesis and DSC study a new pyridinedicarboximide diones derivatives, obtained under various conditions

Krzy

2014

J Therm Anal Calorim

View full text Add to dashboard Cite

The series of three 4-alkoxy-2-[2-hydroxy-3-(4-aryl-1-piperazinyl)propyl]-6-methyl-1H-pyrrolo [3,4-c] pyridine-1,3(2H)-diones were synthesized. The structures of all formed compounds were identified by elemental analysis, FTIR, and 1 H NMR. The synthesized compounds were studied using differential scanning calorimetry and thermogravimetric analysis in order to determine the existence of multiple solid-state forms. Our measurements showed that the solvent, mechanical treatment, and quenching are the important factors. Two stable and one metastable modification were detected. Additionally, DFT calculations were performed.

show abstract

Novel 3-(2-thienyl) acrylic acid bridge di-triphenyltin(IV) {[(Ph)3SnCl)2COO]-[Et3NH]+, [(Ph)3SnCl2)]-[Et3NH]+} complex: XRD/HSA-interactions, physicochemical, thermal and POM/antifungal evaluation

Dahmani¹,

Titi²,

Et-Touhami³

et al. 2023

Inorganica Chimica Acta

View full text Add to dashboard Cite

Thermal analysis of new dimethyl/dibutyl tin(IV) compounds with amino acids

Cited by 7 publications

References 25 publications

The structure–activity relationship of some hexacoordinated dimethyltin(IV) complexes of fluorinated β‐diketone/β‐diketones and sterically congested heterocyclic β‐diketones

The structure–activity relationship of some hexacoordinated dimethyltin(IV) complexes of fluorinated β‐diketone/β‐diketones and sterically congested heterocyclic β‐diketones

Synthesis and DSC study a new pyridinedicarboximide diones derivatives, obtained under various conditions

Novel 3-(2-thienyl) acrylic acid bridge di-triphenyltin(IV) {[(Ph)3SnCl)2COO]-[Et3NH]+, [(Ph)3SnCl2)]-[Et3NH]+} complex: XRD/HSA-interactions, physicochemical, thermal and POM/antifungal evaluation

Contact Info

Product

Resources

About