1981
DOI: 10.1016/0165-2370(81)80024-1
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Thermal degradation of organic polymers using different metals as the pyrolysis filament

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Cited by 16 publications
(4 citation statements)
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“…The pyroprobe uses a resistively heated platinum ribbon (2.1 mm × 35 mm × 0.1 mm) with the ability to heat at rates up to 20 000 °C s –1 . On the basis of previous work in other laboratories, platinum is not acting as a catalyst during the pyrolysis experiments. , Roughly tens to hundreds of micrograms of sample were loaded onto the platinum ribbon and held onto the surface via electrostatic attractions. This method of loading of the ribbon resulted in a submonolayer of sample on its surface.…”
Section: Methodsmentioning
confidence: 99%
“…The pyroprobe uses a resistively heated platinum ribbon (2.1 mm × 35 mm × 0.1 mm) with the ability to heat at rates up to 20 000 °C s –1 . On the basis of previous work in other laboratories, platinum is not acting as a catalyst during the pyrolysis experiments. , Roughly tens to hundreds of micrograms of sample were loaded onto the platinum ribbon and held onto the surface via electrostatic attractions. This method of loading of the ribbon resulted in a submonolayer of sample on its surface.…”
Section: Methodsmentioning
confidence: 99%
“…10 The degraded components of the polymer chain orient randomly during the repolymerization mechanism to rebuild the polymer chains. 13,14 The obtained structures are chemically similar to the bulk polymer units. The thickness of the thin film is largely dictated by the deposition time, 15 while the degradation of polymer chains substantially depends on the heating rate.…”
Section: Introductionmentioning
confidence: 65%
“…It is reported that the fabrication of polymer thin films by evaporation (chemical or physical) is essentially thermal degradation of polymer chains in vacuum, followed by evaporation and repolymerization at the substrate . The degraded components of the polymer chain orient randomly during the repolymerization mechanism to rebuild the polymer chains. , The obtained structures are chemically similar to the bulk polymer units. The thickness of the thin film is largely dictated by the deposition time, while the degradation of polymer chains substantially depends on the heating rate.…”
Section: Introductionmentioning
confidence: 99%
“…Furthermore, heat and mass transfer in thermal analysis seriously affect the kinetics of the reactions and have become even more crucial for fast heating experiments. Low mass and slow heating rate experiments are generally considered free from artifacts due to heat and mass transfer [27,28], although this statement is not always fully satisfied [18].…”
Section: Previous Kinetic Investigationsmentioning
confidence: 99%