Thermogravimetric Pyrolysis of Ammonium and Alkali Metal Tetraphenylborates

Wendlandt, W.W.

doi:10.1021/ac60114a021

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1958

1989

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Cited by 13 publications

(2 citation statements)

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“…The ammonium was precipitated, but when the precipitate was heated it was volatilized. thermal decomposition of the same salt was reported (10) in a thermogravimetric study. It was believed that the thermal decomposition product was KB02.…”

Section: Resultssupporting

confidence: 60%

The Use of 1,3-Dimethylvioluric Acid in Spectrophotometric Titrations of Alkali and Alkaline Earth Salts.

Taylor¹,

Robinson²

1962

Anal. Chem.

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°Average values, using calibration curve prepared in absence of U.region of 1 Mg. of technetium. However, this blank, if not corrected for, nullifies a negative error at higher technetium levels, which is probably due to oxidation of the technetium (V) thiocyanate. Consequently, reasonably accurate results are obtained in the presence of a limited amount of nitrate.Above 6% nitrate, the thiocyanate in the extract deteriorates too rapidly to permit accurate measurement of absorb-

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