Thioasparagine and derivatives for peptide synthesis. A trifluoroacetic acid catalyzed anisyl transfer to sulfur

Ressler, Charlotte; Banerjee, Some Nath

doi:10.1021/jo00870a010

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Scheme 1 Reagents and Conditions1

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2017

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Cited by 15 publications

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“…The filtrates were concentrated under reduced pressure, affording the monoderivatized poly(ethylene glycol) compounds 8-11 with good yields (Table 1) without further purification procedures. As previously reported, 33 treatment of a thioacyl compound with basic conditions can lead to the dithiosulfide derivative as the only product. We investigated the structure of compound 11 and found that it was the dithiosulfide derivative.…”

Section: Scheme 1 Reagents and Conditionssupporting

confidence: 56%