“…Their special sphere architectures provide a wide spectrum of applications such as drug delivery [24], Li ion batteries [25,26], and electro-catalysis [27]. To date, several Co 3 O 4 micro/nano microspheres have been prepared by different methods including hydrothermal synthesis (HS) [24,28], solvothermal synthesis [29], template-assisted electro-deposition [7], and chemical precipitation [30,31], and improved electrochemical/chemical properties have been proven in these systems. Inspired by these works, we report a facile template-free method, chemical bath deposition (CBD), for the fabrication of Co 3 O 4 microspheres consisting of interconnected nanoflakes.…”