Totalsynthese des Enzyminhibitors Spirastrellolid A – Bestätigung der Konfiguration

Perkins, Michael V.

doi:10.1002/ange.200800486

Angewandte Chemie

2008

DOI: 10.1002/ange.200800486

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Totalsynthese des Enzyminhibitors Spirastrellolid A – Bestätigung der Konfiguration

Michael V. Perkins

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Cited by 7 publications

References 23 publications

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Total Synthesis of Spirastrellolide F Methyl Ester—Part 1: Strategic Considerations and Revised Approach to the Southern Hemisphere

et al. 2009

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Um eine optimale Konvergenz bei der vorgesehenen Totalsynthese von Spirastrellolid F zu gewährleisten, wurde der die südliche Hemisphäre repräsentierende Baustein mit einer freien Carbonsäure und einem Enoltriflat‐Terminus hergestellt (siehe Bild). Dieses ungewöhnliche Muster ermöglicht den Aufbau des 38‐gliedrigen makrocyclischen Kerns der Zielstruktur und minimiert die Zahl von Schutzgruppenmanipulationen gegen Ende der Syntheseroute.

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Total Synthesis of Spirastrellolide F Methyl Ester—Part 1: Strategic Considerations and Revised Approach to the Southern Hemisphere

et al. 2009

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A Second‐Generation Total Synthesis of Spirastrellolide A Methyl Ester

Paterson¹,

Maltas²,

Dalby³

et al. 2012

Angewandte Chemie

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Marine Makrolide: Eine verbesserte Totalsynthese zweiter Generation des zytostatischen Makrolids Spirastrellolid‐A‐methylester wurde entwickelt. Die Synthese zeichnet sich durch einen einheitlich hohen Grad an Stereokontrolle sowie eine vereinfachte Fragmentkupplung aus, und der entscheidende Makrolactonisierungsschritt hängt gravierend vom Substitutionsmuster der Linker‐Region C22–C24 ab.

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Total Synthesis of Spirastrellolide F Methyl Ester—Part 1: Strategic Considerations and Revised Approach to the Southern Hemisphere

et al. 2009

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Totalsynthese des Enzyminhibitors Spirastrellolid A – Bestätigung der Konfiguration

Cited by 7 publications

References 23 publications

Total Synthesis of Spirastrellolide F Methyl Ester—Part 1: Strategic Considerations and Revised Approach to the Southern Hemisphere

Total Synthesis of Spirastrellolide F Methyl Ester—Part 1: Strategic Considerations and Revised Approach to the Southern Hemisphere

A Second‐Generation Total Synthesis of Spirastrellolide A Methyl Ester

Total Synthesis of Spirastrellolide F Methyl Ester—Part 1: Strategic Considerations and Revised Approach to the Southern Hemisphere

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