“…2 and 4, the Ni doped samples show spin glass behavior as temperature decreases, indicating the first one might be applicable in our sample. In fact, the existence of spin glass interfaces have been demonstrated in shell-structure g-Fe 2 O 3 /Fe 3 O 4 nanoparticles [7], Fe/g-Fe 2 O 3 nanoparticles [28,29]. Therefore, for the x ¼0.015 sample, the mechanism of unidirectional anisotropy is probably due to the exchange coupling at the interfaces of between the FM regions (phase 2) and the surrounding SG regions.…”