Ultrasound-Assisted and One-Pot Synthesis of New Fe3O4/Mo-MOF Magnetic Nano Polymer as a Strong Antimicrobial Agent and Efficient Nanocatalyst in the Multicomponent Synthesis of Novel Pyrano[2,3-d]pyrimidines Derivatives

Abdtawfeeq, Tarik Hafdhi; Farhan, Zainab A.; Al-Majdi, Kadhum; Jawad, Mohammed Abed; Zabibah, Rahman S.; Riadi, Yassine; Hadrawi, Salema K.; AL-Alwany, Ameen; Shams, Marwah A.

doi:10.1007/s10904-022-02514-7

Cited by 19 publications

(21 citation statements)

References 62 publications

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“…Magnetic, biological, and antimicrobial activities on gram-negative, gram-positive, and fungal strains supported on MFC, MBC, and MIC values are exciting features of this nanopolymer catalyst (Scheme 73). 86 The ultrasound-assisted synthesis of Fe 3 O 4 /Mo-MOF as a nanopolymer was performed in one step. First, H 2 O/ acetic acid (1:1) was added to Fe 3 O 4 -nanoparticles in the presence of dipicolinic acid/MoCl 5 and stirred at 80 C (15 min), and then placed in an ultrasonic device (370 W, 20 min) to obtain Fe 3 O 4 /Mo-MOF.…”

Section: S C H E M Ementioning

confidence: 99%

“…The mechanism for producing compounds 4 is mentioned in Scheme 72. 86 In 2022, Harun Achmad and his colleague used a novel Yttrium-metal-organic framework (Y-MOF) in the synthesis of new pyrazolopyranopyrimidines by MCRs of BA 1, aryl aldehydes 2, hydrazine hydrate 15, and EAA 16 at 50 C in water/ethanol (Scheme 74). In addition, the applications and properties of Y-MOF, and its anticancer activities on breast cancer cells were confirmed based on the MTT procedure.…”

Section: S C H E M Ementioning

confidence: 99%

“…Magnetic, biological, and antimicrobial activities on gram‐negative, gram‐positive, and fungal strains supported on MFC, MBC, and MIC values are exciting features of this nanopolymer catalyst (Scheme 73). 86 …”

Section: Metal–organic Scaffolding Nanocatalyst In the Formation Of H...mentioning

confidence: 99%

“…First, H 2 O/acetic acid (1:1) was added to Fe 3 O 4 ‐nanoparticles in the presence of dipicolinic acid/MoCl 5 and stirred at 80°C (15 min), and then placed in an ultrasonic device (370 W, 20 min) to obtain Fe 3 O 4 /Mo‐MOF. The mechanism for producing compounds 4 is mentioned in Scheme 72 86 …”

Section: Metal–organic Scaffolding Nanocatalyst In the Formation Of H...mentioning

confidence: 99%

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Recent progress of nanocatalyst in the synthesis of heterocyclic compounds by barbituric acids

Safari,

Poursattar Marjani,

Sadrmohammadi

2023

Applied Organom Chemis

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Heterocycles and barbituric acid analogs are particularly used in developing and designing new drugs because of their versatile binding properties for different biotargets. They are present in many natural compounds, vitamins, drugs, and biologically active molecules such as anticancer, antibiotic, antidiabetic, anti‐inflammatory, antidepressant, anti‐HIV, antimicrobial, and insecticidal agents. Using co‐friendly techniques under nanocatalyst conditions drives the synthesis of these bioactive compounds toward green chemistry. This review will investigate the nanocatalysts, including magnetic nanocatalysts, nano metal‐based catalysts, organo‐nanocatalysts, and metal–organic frameworks (MOFs) nanocatalysts employed in the synthesis and design of heterocyclic compounds by barbituric acids from 2017 to 2022.

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Section: S C H E M Ementioning

confidence: 99%

Section: S C H E M Ementioning

confidence: 99%

Section: Metal–organic Scaffolding Nanocatalyst In the Formation Of H...mentioning

confidence: 99%

Section: Metal–organic Scaffolding Nanocatalyst In the Formation Of H...mentioning

confidence: 99%

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Recent progress of nanocatalyst in the synthesis of heterocyclic compounds by barbituric acids

Safari,

Poursattar Marjani,

Sadrmohammadi

2023

Applied Organom Chemis

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“…[29] As a result, sonochemistry is becoming increasingly popular in organic synthesis and has the potential to transform the way organic compounds are synthesized. [30] The synthesis of heterocycles has long been recognized as a critical area within the field of chemistry. [31] These heterocycles are unique organic structures that contain at least one heteroatom other than carbon, giving these compounds special biological and chemical activities.…”

Section: Introductionmentioning

confidence: 99%

Synthesis of Pyrano[2,3‐d]pyrimidine Derivatives Catalyzed by Trimetallic Multi‐walled Carbon Nanotubes under Ultrasound Irradiation Conditions

Harooni,

Naeimi,

Ghasemi

2023

ChemistrySelect

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This study involves the synthesis of pyrano]2,3‐d[pyrimidine derivatives using the multi‐component reactions (MCRs) under ultrasonic, and nanocatalysis conditions. The reaction efficiency was increased and the reaction time was reduced by using a prepared catalyst accomplished with sonication synergetic effect. Furthermore, the increase in product yield can be due to the synergistic property between metals on the surface of the catalyst. This catalyst was found to be recoverable and highly stable under ultrasonic conditions. The use of trimetallic multi‐walled carbon nanotubes (MWCNTs) proved to be highly effective in synthesis of the pyrano[2,3‐d]pyrimidine derivatives. This is due to their active site, economical catalyst loading, easy workup, reusability, and green reaction conditions. Also, the synthesized products were achieved in excellent yields and short reaction times. Different methods were utilized to characterize the nanocatalyst such as; Fourier‐transform infrared spectroscopy (FT‐IR), X‐ray powder diffraction (XRD), field emission scanning electron microscope (FE‐SEM), energy‐dispersive X‐ray spectroscopy (EDS), thermogravimetric analysis (TGA), and the hot filtration method. The synthesized organic compounds were identified through analyses using the melting point, FT‐IR method, and hydrogen‐1 nuclear magnetic resonance (1H NMR).

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The Anticancer, Anti-metastatic, Anti-oxidant, and Anti-angiogenic Activity of Chitosan-coated Parthenolide/Bovine Serum Albumin Nanoparticles

Albosultan

Ghobeh²,

Tabrizi³

2023

J Inorg Organomet Polym

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Ultrasound-Assisted and One-Pot Synthesis of New Fe3O4/Mo-MOF Magnetic Nano Polymer as a Strong Antimicrobial Agent and Efficient Nanocatalyst in the Multicomponent Synthesis of Novel Pyrano[2,3-d]pyrimidines Derivatives

Cited by 19 publications

References 62 publications

Recent progress of nanocatalyst in the synthesis of heterocyclic compounds by barbituric acids

Recent progress of nanocatalyst in the synthesis of heterocyclic compounds by barbituric acids

Synthesis of Pyrano[2,3‐d]pyrimidine Derivatives Catalyzed by Trimetallic Multi‐walled Carbon Nanotubes under Ultrasound Irradiation Conditions

The Anticancer, Anti-metastatic, Anti-oxidant, and Anti-angiogenic Activity of Chitosan-coated Parthenolide/Bovine Serum Albumin Nanoparticles

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