1964
DOI: 10.1007/bf02667025
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Use of rubber columns for the chromatographie separation of triglycerides and other non‐polar compounds

Abstract: Some applications of rubber powder as a sta‐tionary phase in the Chromatographie separation of relatively nonpolar compounds are described. Evidence of a substantial degree of separation of triglyceride components in coconut oil and linseed oil is obtained using a mixture of methanol and acetone as the mobile phase. Separations of trilaurin from mono and dilaurin, of methyl esters of coconut oil fatty acids and of compo‐nents in Oil of Petitgrain are also accomplished.

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Cited by 14 publications
(3 citation statements)
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“…Ion-exchange columns have been proposed for salting-out chromatography (1857), and rubber (2103) or silanized Celite (171) for reversed-phase partition chromatography. The application of cellulose (2026, 2296), polystyrene crosslinked with divinylbenzene (2088), Sephadex (2238), and methylated Sephadex Addition of traces of 4-methyl-2,6-diierf-butylphenol to solvents prevents autoxidation of lipids during chromatography (2276).…”
Section: Alkaloids Both Macekmentioning
confidence: 99%
“…Ion-exchange columns have been proposed for salting-out chromatography (1857), and rubber (2103) or silanized Celite (171) for reversed-phase partition chromatography. The application of cellulose (2026, 2296), polystyrene crosslinked with divinylbenzene (2088), Sephadex (2238), and methylated Sephadex Addition of traces of 4-methyl-2,6-diierf-butylphenol to solvents prevents autoxidation of lipids during chromatography (2276).…”
Section: Alkaloids Both Macekmentioning
confidence: 99%
“…Trowbridge et al (142) rPcoinmended the use of rubber powder chromatographic columns. Swartout and Gross (138) found that triglycerides may be separated by ascending chromatography on uncoated glass fiber filter paper or silica gel coated paper using pyridine-water solvent system.…”
Section: Oils a N D Fatty Acidsmentioning
confidence: 99%
“…Five significant papers concerned the separation of triglycerides. Trowbridge et al (142) recommended the use of rubber powder chromatographic columns.…”
Section: Oils and Fatty Acidsmentioning
confidence: 99%