The urgent need for timely and accurate precipitation estimations in the face of ongoing climate change and the increasing frequency and/or intensity of extreme weather events underscores the necessity for innovative approaches. Recently, several studies have focused on estimating the precipitation rate through induced attenuation of radio frequency (RF) signals, which are abundant in modern communication systems. Most research has concentrated on frequencies exceeding 10 GHz, as attenuation at lower frequencies is minimal, posing measurement challenges. This study aims to confront this limitation by introducing a high-precision experimental setup capable of detecting this subtle attenuation at frequencies under 10 GHz. The setup includes a transmitter and receiver optimized for operation at 2.07, 4.63, and 6.22 GHz, where minimal worldwide research exists. A power resolution below 10−5 dB in preliminary measurements demonstrated its effectiveness in quantifying signal attenuation due to precipitation across the specified frequencies. Moreover, a strong power law relationship was observed between signal attenuation and precipitation rate for all three frequencies, while, as expected, the higher the frequency, the more pronounced the signal attenuation was.