Valorization of Elderberry Pomace using Emerging High-Pressure Technologies: Separation of Compounds with Different Polarities using Subcritical H2O, Supercritical CO2, and CO2/H2O/EtOH Mixture

Mutavski, Zorana; Nastić, Nataša; Fernández, Naiara; Živković, Jelena; Šavikin, Katarina; Vujisić, Ljubodrag; Veberič, Robert; Medič, Aljaž; Vidović, Senka

doi:10.1007/s11947-024-03636-1

Food Bioprocess Technol

2024

DOI: 10.1007/s11947-024-03636-1

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Valorization of Elderberry Pomace using Emerging High-Pressure Technologies: Separation of Compounds with Different Polarities using Subcritical H2O, Supercritical CO2, and CO2/H2O/EtOH Mixture

Zorana Mutavski,

Nataša Nastić,

Naiara Fernández

et al.

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Cited by 1 publication

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CO2-Based Encapsulation of Rutin-Rich Extracts from Black Elderberry Waste Using Advanced PGSS Process

Mutavski,

Vidović,

Ambrus

et al. 2024

Foods

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For the first time, rutin-rich extracts from black elderberry waste (BEW) were encapsulated using the particles from gas-saturated solutions (PGSS) method to improve the preservation of rutin. The extracts used in this study were obtained using five different extraction techniques under optimal conditions, as follows: conventional solid–liquid extraction (SLE) and four non-conventional techniques—ultrasound-assisted extraction (UAE), microwave-assisted extraction (MAE), enhanced solvent extraction (ESE), and supercritical CO2 pretreatment—followed by ESE (SFE-CO2 + ESE). The PGSS process of the obtained extracts was performed using two amphiphilic carriers, glycerol monostearate (GlyMS) and gelucire (Gel), in a mass ratio of 1:6, in favor of the carrier. The efficiency of the PGSS process was evaluated based on the encapsulation yield (EnY), encapsulation efficiency (EE), and physical properties of the encapsulated extracts. The results showed that the SLE extract encapsulated with GlyMS had the highest EnY (92.47%). The Gel only in combination with the ESE extract exceeded the 50% efficacy threshold, with an EnY of 55.18%. The encapsulated SLE extract with Gel showed excellent flow properties and the highest EE (98.91%). These results emphasize the advantages of the PGSS process, including its efficiency and adaptability to produce encapsulated rutin-enriched BEW extracts for pharmaceutical, nutraceutical, and cosmetic applications.

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CO2-Based Encapsulation of Rutin-Rich Extracts from Black Elderberry Waste Using Advanced PGSS Process

Mutavski,

Vidović,

Ambrus

et al. 2024

Foods

View full text Add to dashboard Cite

show abstract

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Valorization of Elderberry Pomace using Emerging High-Pressure Technologies: Separation of Compounds with Different Polarities using Subcritical H2O, Supercritical CO2, and CO2/H2O/EtOH Mixture

Cited by 1 publication

References 49 publications

CO2-Based Encapsulation of Rutin-Rich Extracts from Black Elderberry Waste Using Advanced PGSS Process

CO2-Based Encapsulation of Rutin-Rich Extracts from Black Elderberry Waste Using Advanced PGSS Process

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