2024
DOI: 10.1021/acs.inorgchem.4c01748
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Vanadium-Silsesquioxane Nanocages as Heterogeneous Catalysts for Synthesis of Quinazolinones

Qi Shen,
Kai Sheng,
Zhi-Yong Gao
et al.

Abstract: The functionalization of polyoxovanadate clusters is promising but of great challenge due to the versatile coordination geometry and oxidation state of vanadium. Here, two unprecedented silsesquioxane ligandprotected "fully reduced" polyoxovanadate clusters were fabricated via a facial solvothermal methodology. The initial mixture of the two polyoxovanadate clusters with different colors and morphologies (green plate V 14 and blue block V 6 ) was successfully separated as pure phases by meticulously controllin… Show more

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