The sections in this article are
Introduction
Infrastructure for High‐pressure Experiments
Location
Gas Supply, Compression, and Purification
High‐pressure Reactors
Materials of Construction for High‐pressure Reactors
Metal Components
Sealing Materials
Reactor Design
General Considerations
Pressure Vessels for Batch Processing
Continuous Flow Reactors
Auxiliary Equipment and Handling
Tubes and Fittings
Valves
Pressure Transmitter and Manometer
Reactor Heating and Temperature Control
Stirrer Types
Optical Windows
Pressure Safety Valves and Bursting Discs
Online Sampling
Inline Spectroscopic Measurements
Reactor Cleaning
Cleaning with Organic Solvents
Cleaning with Heated Solvents
Cleaning with Acids
Cleaning with a Combination of Organic Solvent and
sc
CO
2
Dosage Under a High‐pressure Regime
Dosage of Gases
Safety Warnings
Dosing in Batch Processes
Dosage for Continuous Flow Processes
Dosage of Liquids
Dosage of Solids
Further Regulations and Control in Flow Systems
Supply Pressure
Reactor Pressure
Flow and Total Volume Measurement of Depressurized Gas Streams
Evaporation and Condensation
Evaporation
Condensation
Complete Reactor Systems for Synthesis with SCFs
Standard Batch Reactor System
Essential equipment
Brief Description of Work Steps
Fully Automated System for Continuous Flow Operation
Conclusion