Vapor Phase Dehydration of 1-Heptanol over Activated Alumina

Appleby, W. G.; Dobratz, C. J.; Kapranos, S. W.

doi:10.1021/ja01239a043

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1948

1954

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Cited by 10 publications

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“…Isomerization during olefin preparation by dehydration reactions has been reported frequently,1,-16 while many cases have been reported where little or no isomerization occurred. [17][18][19][20] Asinger16 found general isomerization of the double bond all along the carbon chain when dodecanol was dehydrated over alumina at 370-380°or with metaphosphoric acid. Isomerization was observed with alumina at temperatures as low as 250°where the dehydration reaction was incomplete.…”

Section: Resultsmentioning

confidence: 99%

Preparation of 1-C¹⁴-Propene-1 and the Mechanism of Permanganate Oxidation of Propene¹

Fries¹,

Calvin²

1948

J. Am. Chem. Soc.

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Section: Resultsmentioning

confidence: 99%

Preparation of 1-C¹⁴-Propene-1 and the Mechanism of Permanganate Oxidation of Propene¹

Fries¹,

Calvin²

1948

J. Am. Chem. Soc.

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“…of mercury), (2) 22-hour period at 302°C. and constant flow rate, (3) four feed rates at 302°C ., (4) four feed rates at 318 °C., (5) four feed rates at 339°C ., (6) four feed rates at 358°C ., (7) two feed rates at 339°C ., (8) two feed rates at 318°C ., and (9) two feed rates at 302°C. Each condition of temperature and feed rate was maintained for 4 hours.…”

Section: Apparatusmentioning

confidence: 99%