1986
DOI: 10.1002/jpln.19861490313
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Verbessertes Druckaufschlußsystem für biologische und anorganische Materialien

Abstract: Fur die Untersuchung von Nadel-, Blatt-, Holz-, Rinden-, Wurzel-, Boden-und Gesteinsproben zur Klarung der Spurenstoffkreislaufe in Waldokosystemen wurde ein AufschluRsystem benotigt, das folgende Anforderungen erfiillt: a) einfache Handhabung b) geringe Kontaminationen c) Verwendbarkeit fiir unterschiedliche Probenmaterialien und Sauremischungen (HNO3, HNOdHF, HzSOdHF, HN03/H2SOdHF und unter ganz bestimmten Voraussetzungen HN03/HC104/HF und HClOdHF) d) geringe Kosten. Aufbauend auf einer uber zehnjahrigen Erf… Show more

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Cited by 180 publications
(88 citation statements)
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“…Accuracy of the initial ICP-OES results was checked by digestion and analysis of a subset of 28 samples at IOW together with the international reference material SGR-1b (USGS). A total of 50 mg of dried and ground sediment was first treated in open Teflon vessels (PDS-6; Heinrichs et al, 1986) with 1 mL HNO 3 (65 %) at 60 • C for 1 h to oxidize OM. After addition of 2 mL concentrated HF and 2 mL concentrated HClO 4 , the closed vessels were heated at 180 • C for 12 h. After evaporation of the acids on a hot plate at 180 • C, the digestions were fumed off 3 times with 6 M HCl, re-dissolved in 25 ml 2 vol % HNO 3 , and finally measured by ICP-OES (iCAP 7300 Duo, Thermo Fisher Scientific) for K and Ti using Sc as internal standard.…”
Section: Major and Trace Element Contentsmentioning
confidence: 99%
“…Accuracy of the initial ICP-OES results was checked by digestion and analysis of a subset of 28 samples at IOW together with the international reference material SGR-1b (USGS). A total of 50 mg of dried and ground sediment was first treated in open Teflon vessels (PDS-6; Heinrichs et al, 1986) with 1 mL HNO 3 (65 %) at 60 • C for 1 h to oxidize OM. After addition of 2 mL concentrated HF and 2 mL concentrated HClO 4 , the closed vessels were heated at 180 • C for 12 h. After evaporation of the acids on a hot plate at 180 • C, the digestions were fumed off 3 times with 6 M HCl, re-dissolved in 25 ml 2 vol % HNO 3 , and finally measured by ICP-OES (iCAP 7300 Duo, Thermo Fisher Scientific) for K and Ti using Sc as internal standard.…”
Section: Major and Trace Element Contentsmentioning
confidence: 99%
“…The plants were irrigated as necessary. The elemental composition and pH of the experimental plots were determined at harvest by analyzing soil from amended and untreated plots by inductively coupled plasma optical emission spectrometry (Spectro Analytical Instrument, GmbH, Boschstrasse, Kleve, Germany, as described by Heinrichs et al 1986) Gafur et al 2004). For the liquid culture, agar and malt extract were omitted from the medium.…”
Section: Plant Materials and Air Exposure After Root Liftingmentioning
confidence: 99%
“…At each harvest, shoots were separated from roots by cutting with scissors and the plant parts dried at 105°C (24 h). The dried samples were weighed, ground, and a subsample (200 mg) was digested with 4 mL HNO 3 (65 %) at 180°C under pressure (1.0-1.7 MPa) in an oven for 10 h (Heinrichs et al 2007). Digests were analyzed for Cd concentration using flame atomic absorption spectroscopy FAAS.…”
Section: Introductionmentioning
confidence: 99%