Vibrational Absorption

Parson, Walther; Burda, Clemens

doi:10.1007/978-3-031-17222-9_6

Modern Optical Spectroscopy 2023

DOI: 10.1007/978-3-031-17222-9_6

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Vibrational Absorption

Walther Parson

Clemens Burda²

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2024

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Cited by 1 publication

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Elucidation of the Transformation of Coordination Polymer Intermediates into 2D Metal–Organic Framework Films during Chemical Vapor Deposition

Choe,

Park,

Choi

2024

Inorg. Chem.

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Chemical vapor deposition (CVD) is a rising tool to synthesize metal−organic framework (MOF) films. Despite growing interest and usage, its mechanism is less known. Especially, the identification of intermediates is crucial for understanding the growth mechanism and further controlling their structures. In this paper, we investigated the growth mechanism of 2D MOF Cu 3 (C 6 O 6 ) 2 film by CVD. We identified a novel intermediate phase: an octahedral coordination polymer that transforms into an edge-on-oriented 2D MOF. In situ grazing-incidence wide-angle X-ray scattering, X-ray absorption near-edge structure, highresolution transmission electron microscopy, and Raman spectroscopy studies confirmed that this transformation involves the removal of pillars, leading to the formation of a square-planar 2D MOF. With the identification of intermediates, our study deepens the understanding of MOF film formation by CVD, which lays a foundation to control the structure.

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Elucidation of the Transformation of Coordination Polymer Intermediates into 2D Metal–Organic Framework Films during Chemical Vapor Deposition

Choe,

Park,

Choi

2024

Inorg. Chem.

View full text Add to dashboard Cite

show abstract

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Vibrational Absorption

Cited by 1 publication

References 158 publications

Elucidation of the Transformation of Coordination Polymer Intermediates into 2D Metal–Organic Framework Films during Chemical Vapor Deposition

Elucidation of the Transformation of Coordination Polymer Intermediates into 2D Metal–Organic Framework Films during Chemical Vapor Deposition

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