2024
DOI: 10.21203/rs.3.rs-4629665/v1
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Visible-Light-Promoted Direct Desulfurization of Glycosyl Thiols to Access of C-Glycosides

Xiaofeng Ma,
Demeng Xie,
Wei Zeng
et al.

Abstract: C-Glycosides are essential for the study of biological processes and the development of carbohydrates-based drugs. Despite tremendous hurdles, glycochemists have often fantasized of the efficient, highly stereoselective synthesis of C-glycosides with the shortest steps under mild conditions. Herein, we report a desulfurative radical protocol to synthesize C-alkyl glycosides and coumarin C-glycosides under visible-light induced conditions without the need of an extra photocatalyst, in which stable and readily a… Show more

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