This paper describes combined rheological, ballistic, and optical analyses performed on para©n-based mixtures that can be used as high regression rate hybrid rocket fuels. Experimental activities have been done at the DLR Institute of Space Propulsion in Lampoldshausen and at SPLab of Politecnico di Milano [1]. Herein, the experiments that were performed at the DLR are described in detail. Viscosity, surface tension, and regression rate of the fuels have been determined. Furthermore, the combustion was evaluated by optical measurements. Data collected so far indicate an increasing regression rate for decreasing viscosity of the liquid para©n which is in accordance with the current theories. Droplet entrainment, which is related to high regression rates, is only visible for the low-viscosity para©n-based fuels.