Volumetric Determination of Iron and Titanium

Determination of Iron in Presence of Chromium and Titanium with Jones Reductor

“…That simple air-oxidation of a titanous solution is not dependable is shown by McNabb and Skolnik (7). Their results corroborate the experience of Margaret D. Foster of this laboratory, who found that in a solution containing titanous salt equivalent to 0.04 gram of titanium dioxide less than three fourths of the titanium was reoxidized to the quadrivalent state after 10 hours of aeration; a solution containing 0.09 gram of titanium dioxide was less than nine-tenths converted in the same time.…”

“…McNabb and Skolnik (7) found that the addition of 50 ml. of saturated mercuric chloride solution greatly increased the rate of oxidation of titanous sulfate by aeration.…”