2018
DOI: 10.3897/j.moem.4.1.33272
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X-ray peak profile analysis of CoAl2O4 nanoparticles by Williamson-Hall and size-strain plot methods

Abstract: Citation: Irfan H, Mohamed Racik K, Anand S (2018) X-ray peak profile analysis of CoAl 2 O 4 nanoparticles by Williamson-Hall and size-strain plot methods. Modern Electronic Materials 4(1): 31-40. https://doi. AbstractCoAl 2 O 4 nanoparticles were prepared by a sol-gel process using citric acid as chelating agent with different calcination temperatures of 600 to 900 °C. The crystalline spinel cubic phase was confirmed by X-ray diffraction results. High-resolution scanning electron microscopy (HRSEM) revealed t… Show more

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Cited by 29 publications
(15 citation statements)
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“…In comparison, phase γ(Ni5Zn21) does not exhibit the same behavior that could be associated with its higher stability. It has been stated in the literature [8,[20][21][22] that alloys with a nickel content of 12% consist solely of intermetallic(δ-phase) Ni3Zn22. The improvement in the nickel content by up to 19 at.…”
Section: X-ray Diffractionmentioning
confidence: 99%
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“…In comparison, phase γ(Ni5Zn21) does not exhibit the same behavior that could be associated with its higher stability. It has been stated in the literature [8,[20][21][22] that alloys with a nickel content of 12% consist solely of intermetallic(δ-phase) Ni3Zn22. The improvement in the nickel content by up to 19 at.…”
Section: X-ray Diffractionmentioning
confidence: 99%
“…The deposit prepared at a temperature of 40℃ gives us a uniform and compact pyramidal structure, consisting of several large grain size films. The presence of a pyramidal morphology was due to the greater quantity of zinc in the layer (with an amount of 13% Nickel in the deposit) [21,22]. Increasing the temperature from 70 to 90°C activates the electrodepositing Nickel, which consequently creates a significant amount of nickel in the layers, so the deposit becomes irregular and non-uniform, while some fine cracks occur on the coating surface.…”
Section: Effect Of the Bath Temperaturementioning
confidence: 99%
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“…If the profiles are purely Gaussian or purely voightian, this method provides a very simple and quick way to evaluate the effects of stress and size. For the other pseudo-voighian profiles, approximations are necessary for the separation of these two effects [21,22].…”
Section: Figure 2 Diagram Shape Of Williamson and Hallmentioning
confidence: 99%
“…For the other pseudo-Voightian profiles, approximations are necessary for the separation of these two effects. 21,22…”
Section: Introductionmentioning
confidence: 99%